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Chapter 9

Method Development and Sampling Techniques

Sviluppo di metodi analitici
Sviluppo di metodi analitici
An analytical methodology can be divided into four sequential steps: technique, method, procedure, and protocol. A technique is a scientific principle ...
Controllo qualità
Controllo qualità
Quality control is one of the three cyclical quality assurance activities that help keep a system under statistical control. Typical quality control ...
Garanzia di qualità
Garanzia di qualità
Quality assurance is the overarching term used to describe the activities employed to ensure the proper performance of a system. These activities can be ...
Validazione dei dati
Validazione dei dati
Method validation is a crucial process in analytical chemistry designed to confirm that a given method consistently produces reliable and high-quality ...
Analisi qualitative
Analisi qualitative
Qualitative analysis is the process of identifying elements, ions, or compounds in an unknown sample. It is the first and most fundamental type of ...
Analisi quantitativa
Analisi quantitativa
Quantitative analysis is a technique for measuring the amount of specific constituents in a sample. When the sample's composition is unknown, ...
Taratura dello strumento
Taratura dello strumento
Instrument calibration is essential for ensuring that instruments produce accurate and consistent results. It is vital in manufacturing, healthcare, ...
Taratura della vetreria
Taratura della vetreria
Accurate calibration of glassware, such as volumetric flasks, pipettes, and burettes, is essential to ensure accurate measurements in the analytical ...
Soluzioni standard
Soluzioni standard
Standard solutions refer to solutions with a precisely known concentration or composition. A primary standard is a highly pure, high molar mass, stable ...
Soluzioni cieca
Soluzioni cieca
A blank solution is a solution that does not contain the analyte, or the substance of interest being tested or measured. It is typically prepared using ...
Metodi di campionamento: panoramica
Metodi di campionamento: panoramica
A sample refers to a smaller subset representative of a larger population. In analytical chemistry, studying or analyzing an entire population is often ...
Metodi di campionamento: tipi di campioni
Metodi di campionamento: tipi di campioni
Sampling materials are classified into three main types: solid, liquid, and gas. Solid samples include a variety of substances, such as sediments from ...
Piani di campionamento
Piani di campionamento
Sampling is a crucial step in analytical chemistry, allowing researchers to collect representative data from a large population. Common sampling methods ...
Preparazione del campione per l'analisi: panoramica
Preparazione del campione per l'analisi: panoramica
Sample preparation is an essential step in the analytical process. It involves preparing a sample so that it can be analyzed accurately. The goal is to ...
Preparazione del campione per l'analisi: tecniche avanzate
Preparazione del campione per l'analisi: tecniche avanzate
Accurate analysis of complex samples often requires advanced preparation techniques to achieve reliable and reproducible results. Samples containing ...
Gestione dei campioni
Gestione dei campioni
Transportation of samples from the collection point to the laboratory, as well as storage and preservation techniques, are crucial for maintaining sample ...
Contaminanti ed errori
Contaminanti ed errori
Effective sample preparation is crucial for accurate and reliable laboratory analysis. During this process, two significant sources of error can arise: ...
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