Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron Microscope
3.8K Views
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14:21 min
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July 24th, 2021
DOI :
July 24th, 2021
•Kinga A. Unocic1, Dale K. Hensley1, Franklin S. Walden2, Wilbur C. Bigelow3, Michael B. Griffin4, Susan E. Habas4, Raymond R. Unocic1, Lawrence F. Allard5
1Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, 2Protochips Inc., 3Department of Materials Science & Engineering, University of Michigan, 4Catalytic Carbon Transformation & Scale-up, National Renewable Energy Laboratory, 5Materials Science & Technology Division, Oak Ridge National Laboratory
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Chapters in this video
0:00
Introduction
1:40
E-chip Preparation
5:10
Preparation of the CCGR-TEM Holder
6:23
Preparation of Experimental Setup
7:59
Residual Gas Analyzer (RGA) System
10:52
Running the Reaction
12:46
Representative Results
13:29
Summary
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