24.6K Views
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11:42 min
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May 15th, 2012
DOI :
May 15th, 2012
•0:05
Title
1:55
Loading of First Bis-Peptide, Deprotection of First Bis-Peptide, and Simultaneous Resin Capping
3:43
Coupling Tert-butyl Carbamate (Boc)/tert-butyl Ester(tBu)-protected Functionalized Bis-Amino Acid
5:21
Deprotection of Boc/tBu-protected Functionalized Bis-Amino Acid, Deprotection of Fmoc, and Acylation of the First Bis-Amino Acid
6:55
Removal of the Boc Group from the Resin Bound Amino Acid and Cleavage from the Resin
7:56
Assessment Methods
9:51
Results: Analysis by Liquid Chromatography and Mass Spectroscopy
10:36
Conclusion
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